J/A+A/658/A127      Spectroscopy of CD3OH                    (Ilyushin+, 2022)

Rotational and rovibrational spectroscopy of CD3OH and an account on CD3OH toward IRAS 16293-2422. Ilyushin V.V., Muller H.S.P., Jorgensen J.K., Bauerecker S., Maul C., Bakhmat Y., Alekseev E.A., Dorovskaya O., Vlasenko S., Lewen F., Schlemmer S., Berezkin K., Lees R.M. <Astron. Astrophys. 658, A127 (2022)> =2022A&A...658A.127I 2022A&A...658A.127I (SIMBAD/NED BibCode)
ADC_Keywords: Interstellar medium; Spectra, millimetric/submm; Spectroscopy Keywords: molecular data - methods: laboratory: molecular - techniques: spectroscopic - radio lines: ISM - ISM: molecules - astrochemistry Abstract: Solar-type protostars have been shown to harbor highly deuterated complex organics as for example witnessed by the high relative abundances of doubly and triply deuterated isotopologs. While this degree of deuteration may provide important clues to the formation of these species, spectroscopic information on multiply deuterated isotopologs is often insufficient. In particular, searches for triply deuterated methanol, CD3OH, are hampered to a large extent by the lack of intensity information from a spectroscopic model. The aim of the present study is to develop a spectroscopic model of CD3OH in low-lying torsional states sufficiently accurate to facilitate further searches for CD3OH in space. We have performed a new measurement campaign for CD3OH involving three spectroscopic laboratories which covers the 34GHz-1.1THz and the 20-900cm-1 ranges. The analysis was perfomed using the rho-axis-method torsion- rotation Hamiltonian model. We determined a model that describes the ground and first excited torsional states of CD3OH up to quantum numbers J≤55 and K≤23, and derived a line list for radio-astronomical observations. The resulting line list is accurate up to at least 1.1THz and should be sufficient for all types of radio-astronomical searches for this methanol isotopolog. This line list was used to search for CD3OH in data from the Protostellar Interferometric Line Survey of IRAS 16293-2422 using the Atacama Large Millimeter/submillimeter Array. CD3OH is securely detected in the data with a large number of clearly separated and well-reproduced lines. We detected not only lines belonging to the ground torsional state, but also several belonging to the first excited torsional state. The derived column density of CD3OH and abundance relative to non-deuterated isotopolog confirm the significant enhancement of this multiply deuterated variant. This is in line with other observations of multiply deuterated complex organic molecules and may serve as an important constraint on models for their formation. Description: Table A1 contains assigned microwave transitions of the CD3OH spectrum used in the analysis. Source of data: Khark - Kharkov spectrometer, present work; Koln - Cologne spectrometers, present work; for other source codes (B,C,D,F) see Walsh M.S., Xu L.-H., & Lees R.M. 1998, J. Mol. Spectrosc., 188, 85. Table A2 contains assigned FIR transitions of the CD3OH spectrum used in the analysis. Source of data: Braunschweig measurements, present work. Table A3 contains predicted transitions of the ground and first excited torsional states of CD3OH in the frequency range from 1GHz up to 1.3THz with J up to 60 and |Ka| up to 24. The m values 0/1 and -3/-2 correspond to A/E transitions of the vt=0 and 1 torsional states, respectively. We limit our calculations to transitions for which uncertainties are less than 0.1 MHz. Table A4 contains torsion-rotation part Qrt(T) of the total internal partition function Q(T)=Qv(T)*Qrt(T), calculated for CD3OH from first principles using the parameter set of Table 2. The vibrational part Qv(T) (omitting the torsional vibration since it is taken into account in Qrt) may be estimated in the harmonic approximation using the vibrational frequencies reported by T. Schimanouchi, Tables of Molecular Vibrational Frequencies, Vol. I: consolidated (National Bureau of Standards, Washington, DC, 1972), pp. 1-160. In the calculation the states up to J=100 and vt=11 were included. File Summary: -------------------------------------------------------------------------------- FileName Lrecl Records Explanations -------------------------------------------------------------------------------- ReadMe 80 . This file tablea1.dat 75 8580 Assigned microwave transitions of the CD3OH spectrum used in the analysis tablea2.dat 71 7218 Assigned FIR transitions of the CD3OH spectrum used in the analysis tablea3.dat 87 24574 Predicted transition frequencies of the ground and first excited torsional states of CD3OH in the frequency range from 1GHz up to 1.3THz tablea4.dat 16 30 Torsion-rotation part Qrt(T) of the total internal partition function Q(T)=Qv(T)*Qrt(T), calculated for CD3OH from first principles (corrected version, 20-Mar-2022) -------------------------------------------------------------------------------- Byte-by-byte Description of file: tablea1.dat -------------------------------------------------------------------------------- Bytes Format Units Label Explanations -------------------------------------------------------------------------------- 1- 2 A2 --- Sym' Upper level symmetry in the G6 group 4- 5 I2 --- m' Upper free rotor torsional quantum number 7- 9 I3 --- J' Upper J quantum number 11- 13 I3 --- Ka' Upper Ka quantum number 15- 17 I3 --- Kc' Upper Kc quantum number 22- 23 A2 --- Sym" Lower level symmetry in the G6 group 25- 26 I2 --- m" Lower free rotor torsional quantum number 28- 30 I3 --- J" Lower J quantum number 32- 34 I3 --- Ka" Lower Ka quantum number 36- 38 I3 --- Kc" Lower Kc quantum number 40- 51 F12.3 MHz Freq Observed transition frequency 54- 59 F6.3 MHz unc Uncertainty of measurement 62- 69 F8.4 MHz O-C Residuals from the fit 72- 75 A4 --- Cmnt Source of data -------------------------------------------------------------------------------- Byte-by-byte Description of file: tablea2.dat -------------------------------------------------------------------------------- Bytes Format Units Label Explanations -------------------------------------------------------------------------------- 1- 2 A2 --- Sym' Upper level symmetry in the G6 group 4- 5 I2 --- m' Upper free rotor torsional quantum number 7- 9 I3 --- J' Upper J quantum number 11- 13 I3 --- Ka' Upper Ka quantum number 15- 17 I3 --- Kc' Upper Kc quantum number 22- 23 A2 --- Sym" Lower level symmetry in the G6 group 25- 26 I2 --- m" Lower free rotor torsional quantum number 28- 30 I3 --- J" Lower J quantum number 32- 34 I3 --- Ka" Lower Ka quantum number 36- 38 I3 --- Kc" Lower Kc quantum number 40- 49 F10.4 cm-1 Freq Observed transition frequency 53- 59 F7.4 cm-1 unc Uncertainty of measurement 63- 71 F9.5 cm-1 O-C Residuals from the fit -------------------------------------------------------------------------------- Byte-by-byte Description of file: tablea3.dat -------------------------------------------------------------------------------- Bytes Format Units Label Explanations -------------------------------------------------------------------------------- 1- 2 A2 --- Sym' Upper level symmetry in the G6 group 4- 5 I2 --- m' Upper free rotor torsional quantum number 7- 9 I3 --- J' Upper J quantum number 11- 13 I3 --- Ka' Upper Ka quantum number 15- 17 I3 --- Kc' Upper Kc quantum number 22- 23 A2 --- Sym" Lower level symmetry in the G6 group 25- 26 I2 --- m" Lower free rotor torsional quantum number 28- 30 I3 --- J" Lower J quantum number 32- 34 I3 --- Ka" Lower Ka quantum number 36- 38 I3 --- Kc" Lower Kc quantum number 40- 52 F13.4 MHz Freq Predicted transition frequency 55- 62 F8.4 MHz unc Predicted uncertainty of transition frequency 66- 75 F10.4 cm-1 Elo The energy of the lower state 78- 87 E10.3 D+2 Sm2 Dipole moment squared multiplied by the transition linestrength and nuclear spin statistical weight -------------------------------------------------------------------------------- Byte-by-byte Description of file: tablea4.dat -------------------------------------------------------------------------------- Bytes Format Units Label Explanations -------------------------------------------------------------------------------- 1- 5 F5.1 K T Temperature 8- 16 F9.2 --- Qrt Torsion-rotation part of the partition function -------------------------------------------------------------------------------- Acknowledgements: Vadim Ilyushin, ilyushin(at)rian.kharkov.ua History: 10-Feb-2022: on-line version 20-Mar-2022: tablea4 corrected (from author)
(End) Vadim Ilyushin [IRA NASU], Patricia Vannier [CDS] 08-Nov-2021
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